Intergranular Corrosion Test (IGC) per ASTM A At TCR Engineering Services, several methods exist for the testing of intergranular corrosion. To conduct. Detecting Susceptibility to Intergranular Attack in Austenitic Stainless Steels. ASTM A is the specification which governs five practices used to determine if the. Abstract. A detailed study of AISI and stainless steels (SSs) has been conducted to correlate the degree of sensitization (DOS) measured by the.
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This practice includes boiling the sample for 24 to hours in the solution above, and measures the materials performance quantitatively.
Our knowledgeable scientists have the experience and expertise necessary to determine the most appropriate intergranular attack testing methods for your material while providing actionable results you can rely on. Where a standard is included in a purchase specification, this must be followed, although it is advised that unsuitable tests, such as the Huey test for duplex and super austenitic stainless steels, are queried. In everyday applications, corrosion varies by materials and solutions.
ASTM G28 method B is a more aggressive test than method A and is intended for more corrosion resistant alloys, as listed in the document. Strauss test specimens are boiled in a Copper Sulfate – Sulfuric Acid mixture for 15 hours. It is the responsibility of the user of this standard to establish appropriate safety and health asgm and determine the applicability aatm regulatory limitations prior to use.
A recent publication on intergranular corrosion. Practice F, is a hour weight-loss based analysis that provides a quantitative measure of the materials performance, and is commonly used to analyze as-received stainless steels.
Where a bend test is required, the sample must be bent over a mandrel of a diameter related to the specimen diameter, without any cracking, as determined by inspection under a low power microscope and a microsection in any suspicious areas.
Classification of structure then provides either acceptance or further testing required, which typically moves you to one of the next practices.
Intergranular Attack – ASTM A – Colorado-Metallurgical-Services
Intergranular simply means that the corrosion is taking place between the grains or crystals, which is where sigma phase or chromium carbides are going to form which makes the material susceptible to IGA.
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These tests are often run as a qualification test to ensure each batch of stainless steel is properly prepared. A bend test followed by a visual or micro-examination are used to determine “Pass” or “Fail” of test specimens.
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For many alloys, the onset axtm at 0. SEP does not require ageing, although it might be required in a specification calling up this standard. All five methods within this specification involve exposing specimens to a chemical mixture designed to encourage corrosive behavior. Similar to the Streicher test, the Huey test method uses a nitric acid solution and subjects the specimen to five hour boiling intervals.
All bend tests require a tensile test machine or similar, with suitable grips and sufficient strength to bend the strongest alloy.
This simple etching technique is used as a quick screening method to ensure that a material is free of intergranular corrosion susceptibility. Just remember that these tests were devised for specific groups of alloys and should not be applied to all CRAs! As 15 atsm is a difficult test period in practice, and is only a minimum, conducting the test for 20 hours overnight means that the two tests are equivalent.
Link to Active This link will always route asrm the current Active version of the standard. If materials with incorrect heat treatment enter service, they are liable to crack or fail by intergranular corrosion IGC much more rapidly than properly treated materials; ASTM A is a screening test to help find batches that are incorrectly processed. For alloys not listed in this standard, it s262 be necessary to carry out some tests on material in various conditions to determine the threshold.
All austenitic stainless steels should meet this requirement, if proper annealing took satm. Rockwell or Superficial Hardness.
Intergranular Corrosion Testing: An Overview of ASTM A262
ISO is specifically for duplex and all austenitic stainless steels, and recommends ageing at two different temperatures: At the conclusion off the test, specimens are either visually examined or measured for weight loss and compared to an established corrosion rate for that specific material type.
None of these are identical and cross substitution of results is not possible.
It does not say what to do about duplex or super austenitic alloys. Both of these tests should be followed by water quenching. Test Samples Samples may be rectangular or cylindrical to suit the test vessel, but where a bend test is required, aastm is suggested that the sample be a minimum of mm long.
The samples are etched after metallographic preparation for cross-sectional examination which is thoroughly viewed with a traverse from inside to outside diameters of rods and tubes, from face to face on plates, and across all zones such as weld metal, weld-affected zones, and base plates 2a62 specimens containing welds.
However, when a material is exposed to high temperatures for long periods of time, a process called sensitization may occur.
We provide intergranular corrosion evaluation, salt spray testing, stress corrosion, and various other methods to simulate exposure of your products or materials to corrosive environments. The test is generally performed for acceptance of materials, but not sufficient for rejection of materials.
ASTM A Intergranular Corrosion Testing and Analysis
Selection of a Test Method The test methods in Table 1 were designed with specific alloys in mind, but the proliferation of new CRAs has meant that the selection of a suitable test method is difficult. The bent samples are examined at low magnification, where the appearance of cracks or fissures indicate intergranular attack. The samples are weighed at each interval to determine mass loss and degree of susceptibility to intergranular attack. It has been used for the duplex stainless steel UNS Swhich has been used for nitric acid cooler tubes.
Duplicate samples from both sides of a sheet sample are evaluated to determine if carburization results in intergranular attack. From macroscopic imaging to Scanning Electron Microscopy, Element provides turnkey metallographic services using state-of-the-art equipment. This test should be avoided for most CRAs, except in the circumstances described below, in section 4.